Category: esters-buliding-blocks. Recently I am researching about ALKYLBORONIC ESTERS; BOND FORMATION; BORYLATION; SECONDARY; SUBSTITUTION; CONSTRUCTION; ACTIVATION; ALKENES; HALIDES, Saw an article supported by the National Key R&D Program of China [2017YFA0303502]; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21572212, 21732006, 21702200, 51821006]; Strategic Priority Research Program of CAS [XDB20000000]; Major Program of Development Foundation of Hefei Centre for Physical Science and Technology [2017FXZY001]. Published in AMER CHEMICAL SOC in WASHINGTON ,Authors: Wang, XX; Li, L; Gong, TJ; Xiao, B; Lu, X; Fuo, Y. The CAS is 103-25-3. Through research, I have a further understanding and discovery of Methyl 3-phenylpropionate
Vicinal diboration of alkyl bromides via tandem catalysis is reported. The reported reaction exhibits a broad substrate scope, good functional group compatibility, and regioselectivity. Moreover, it shows good practicality due to the easy accessibility of alkyl bromides in combination with diverse transformations of diboronates. Mechanism study indicates that terminal alkenes are generated selectively through nickel-catalyzed dehydrohalogenation of alkyl bromides followed by base/MeOH promoted diboration process to provide 1,2-diboration products.
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Reference:
Patent; SANOFI; US2011/294788; (2011); A1;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics