Introduction of a new synthetic route about Methyl 3-phenylpropionate

Adding a certain compound to certain chemical reactions, such as: 103-25-3, name is Methyl 3-phenylpropionate, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 103-25-3, Computed Properties of C10H12O2

Adding a certain compound to certain chemical reactions, such as: 103-25-3, name is Methyl 3-phenylpropionate, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 103-25-3, Computed Properties of C10H12O2

In the 10mL single-mouth bottle,Nitrogen protection,82.1 mg (0.50 mmol) of compound 1e is added,2.5mL n-pentane,105.9 mg (2.25 mmol) deuterated ethanol (EtOD),16.0 mg (2.25 mmol) lithium block,Stir for 5 min at 0C.Rise to room temperatureThe reaction was quenched with 3.0 M aqueous hydrochloric acid.Add ether and saturated salt,59.0 mg of target compound 4a was obtained.Yield 85%.

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Reference:
Patent; China Agricultural University; An Jie; Lei Peng; Han Minhui; Ma Xiaodong; Wu Yufei; A Dila·adijiang; Ding Yuxuan; (15 pag.)CN107445798; (2017); A;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics