Related Products of 140-39-6, The chemical industry reduces the impact on the environment during synthesis 140-39-6, name is p-Tolyl Acetate, I believe this compound will play a more active role in future production and life.
General procedure: A mixture of aryl ester (25 mmol), HFSiO2 (2 g), and EtOAc (5 mL) was charged in a 50 ml flask and stirred for 5min. EtOAc was used for homogenization of the reactionmixture in this step. The solvent was evaporated under vacuumand the residue was heated with the classical method for 4 h at 55C for aryl acetates and at 75C for aryl benzoates(Table 1). After cooling, the reaction mixture was extractedwith EtOAc (3 × 10 mL) and the solvent was removed under vacuum. The residue was subjected to short column chromatography (EtOAc/hexane; 1:5) on silica gel to obtain pureproducts. All the isolated hydroxyaryl ketones successfullygave the related spectral data of IR, 1H NMR, 13C NMR andMS spectrometers (see the Supporting Information, Fig. 12S-39S) and comparison with authentic samples prepared byreported methods [33-36].
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, p-Tolyl Acetate, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Paghandeh, Hossein; Saeidian, Hamid; Ghaffarzadeh, Mohammad; Letters in Organic Chemistry; vol. 15; 9; (2018); p. 809 – 814;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics