Comparative study on the effect of two drying methods on the guest encapsulation behavior of osmanthus flavor-2-hydroxypropyl-β-cyclodextrin inclusion complex was written by Hu, Jing;Du, Peiting;Liu, Shanshan;Liu, Qinghe;Deng, Weijun. And the article was included in Flavour and Fragrance Journal in 2021.Name: 5-Hexyldihydrofuran-2(3H)-one This article mentions the following:
In this study, osmanthus flavor (OF) and HP-β-CD were used to prepare OF and HP-β-CD inclusion complex (OF-CD). OF-CD powders were obtained with oven-drying and freeze-drying, sep. The effect of drying methods was investigated with the morphol. and odor evaluation first. The chem. structure and flavor loading ratio of OF-CDs were determined by Fourier transform IR spectroscopy (FTIR) and Gas chromatog.-mass spectrometry (GC-MS). The flavor was successfully be encapsulated by HP-β-CD forming OF-CD inclusion complex. Oven-drying led to compact blocky solid, while freeze-drying resulted in porous morphol. The amount of flavor in OF-CD with oven-drying (48.61 μg[n.8260]g) was found lower than that in OF-CD with freeze-drying (58.1 μg[n.8260]g). In particular, the content of alcoholics in OF-CD with oven-drying (11.8 μg[n.8260]g) was much lower than that in OF-CD with freeze-drying (19.04 μg[n.8260]g). Thermogravimetric anal. (TGA) showed that the average activation energy of OF-CD with oven-drying (66.3-135.4 kJ mol-1) was higher than OF-CD with freeze-drying (53.0-100.7 kJ mol-1) by 13.3-34.7 kJ mol-1. More intermol. hydrogen bonds in OF-CD with freeze-drying led to high encapsulation of partial components; however, they are not thermostable, resulting in fast release at high temperature The better thermal stability of OF-CD with oven-drying makes itself a better candidate for flavor encapsulation for cooking at high temperature In the experiment, the researchers used many compounds, for example, 5-Hexyldihydrofuran-2(3H)-one (cas: 706-14-9Name: 5-Hexyldihydrofuran-2(3H)-one).
5-Hexyldihydrofuran-2(3H)-one (cas: 706-14-9) belongs to esters. Esters typically have a pleasant smell; those of low molecular weight are commonly used as fragrances and are found in essential oils and pheromones. Cyclic esters are called lactones, regardless of whether they are derived from an organic or inorganic acid. One example of an organic lactone is γ-valerolactone.Name: 5-Hexyldihydrofuran-2(3H)-one
Referemce:
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics