Synthetic Route of 6290-49-9, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 6290-49-9, name is Methyl 2-methoxyacetate belongs to esters-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
In a 1000 ml four-necked flask, 102 g (0.98 mol) of methyl methoxyacetate and 75 g (1.25 mol) of methyl formate were added, and the temperature was lowered to 10 C. with stirring.60 g (1.11 mol) of sodium methoxide was added in portions, and the temperature was controlled to not exceed 30 C.After the addition of sodium methoxide, the reaction was stirred at 25 C for 2h, and the temperature was raised to 36 C for 4h.At the end of the reaction, the temperature was lowered and suction filtered. The solid product content was 98.0%, and the yield was 92.0%.
The synthetic route of Methyl 2-methoxyacetate has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Jiangsu Kuai Da Agrochemical Co., Ltd.; Lin Longlong; Wu Feng; Cao Weidong; Xia Xiaofeng; (4 pag.)CN110759829; (2020); A;,
Ester – Wikipedia,
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