Adding a certain compound to certain chemical reactions, such as: 3196-23-4, name is Methyl 1-bromocyclohexanecarboxylate, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 3196-23-4, HPLC of Formula: C8H13BrO2
A mixture of 3 g of finely chipped zinc, catalytic amount of mercuricchloride, 30 ml of anhydrous benzene, 1 ml of HMPTA, 25 mmol (5.53 g) of methyl 1-bromocyclohexanecarboxylate, and10 mmol (2.03 g) of compound II was boiled for 4 h, cooled, and decanted from the excess zinc; then it was hydrolyzed with5% acetic acid; the organic layer was separated, and the reaction products were twice extracted from the aqueous layer withethyl acetate. When the extract was dried with anhydrous sodium sulfate, the solvents were distilled, and compound III wasrecrystallized from ethanol. The yield was 1.85 g (59%)
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Reference:
Article; Kirillov; Nikifirova; Dmitriev; Baibarodskikh; Journal of Structural Chemistry; vol. 57; 6; (2016); p. 1263 – 1265; Zh. Strukt. Kim.; vol. 57; 6; (2016); p. 1327 – 1329,3;,
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