Adding a certain compound to certain chemical reactions, such as: 35065-86-2, name is 3-Bromophenyl acetate, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 35065-86-2, Recommanded Product: 3-Bromophenyl acetate
Acetylated intermediate and aluminum trichloride (2.3g) with vigorous stirringThe mixture was heated to 160 C under an argon atmosphere for 2 h in a 50 mL single-mouth bottle, cooled to room temperature, and extracted with a 3 M hydrochloric acid solution and ethyl acetate.After the organic phase is washed with water and a saturated sodium chloride solution,Dry over anhydrous sodium sulfate.After concentration, column chromatography gave 1 g of pale yellow solid.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 3-Bromophenyl acetate, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Shanghai Changsen Pharmaceutical Co., Ltd.; Wang Zhe; Fan Guoqin; Zeng Zhihong; Wang Xiaoguang; Jiang Rongzhen; (64 pag.)CN109678796; (2019); A;,
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