Multivariate optimization of dual-sorbent dynamic headspace extraction of volatiles in wine analysis was written by Vyviurska, Olga;Hanobikova, Maria;Gomes, Adriano A.;Spanik, Ivan. And the article was included in Food Chemistry in 2021.Computed Properties of C6H10O2 This article mentions the following:
The main critical point of newly developed miniaturized sample preparation techniques is a limited extraction capacity. Dynamic headspace extraction offers increased volume of sorbent which is commonly used in environmental anal. Application of two sorbents (Carbopack B/Carbopack X and Tenax TA) at different extraction temperatures allows enhancing a range of volatile organic compounds available for anal. Such approach was applied in our research for quantification of volatile organic compounds in botrytized wines with gas chromatog. The central composite design was included to anal. simultaneous effects of incubation time, incubation temperature, purge volume and purge flow. In attempt to properly assess results, the data evaluation involved Pareto charts, surface response methodol. and principal component anal. Multivariate exptl. design revealed statistical significance of purge volume and quadratic terms of incubation time and temperature, for response of volatiles. The quantification method with 0.2-2.0μg/L LOD and 0.5-5.0μg/L LOQ values, was developed under simultaneously optimized exptl. conditions such as a 54°C incubation temperature, a 20.18 min incubation time, a 344.3 mL purge volume and a 16.0 mL/min purge flow. The increased levels of linalool oxide, Et phenylacetate, γ-hexalactone and α-terpineol were observed in the samples, that correlated with botrytized wine technol. In the experiment, the researchers used many compounds, for example, 5-Ethyldihydrofuran-2(3H)-one (cas: 695-06-7Computed Properties of C6H10O2).
5-Ethyldihydrofuran-2(3H)-one (cas: 695-06-7) belongs to esters. Esters are widespread in nature and are widely used in industry. In nature, fats are in general triesters derived from glycerol and fatty acids. Esters are responsible for the aroma of many fruits, including apples, durians, pears, bananas, pineapples, and strawberries. Cyclic esters are called lactones, regardless of whether they are derived from an organic or inorganic acid. One example of an organic lactone is γ-valerolactone.Computed Properties of C6H10O2
Referemce:
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics