I found the field of Chemistry very interesting. Saw the article Nickel salt of phosphomolybdic acid as a bi-functional homogeneous recyclable catalyst for base free transformation of aldehyde into ester published in 2020. Recommanded Product: Methyl 3-phenyl-2-propenoate, Reprint Addresses Patel, A (corresponding author), Maharaja Sayajirao Univ Baroda, Fac Sci, Dept Chem, Polyoxometalates & Catalysis Lab, Vadodara 390002, India.. The CAS is 103-26-4. Through research, I have a further understanding and discovery of Methyl 3-phenyl-2-propenoate
A Ni salt of phosphomolybdic acid (NiHPMA) was synthesized and characterized by various physico-chemical techniques such as EDX, UV-Visible spectroscopy, FT-IR, Raman spectroscopy and XPS. FT-IR and Raman spectroscopy confirm the presence of Ni as a counter cation while UV-Visible and XPS studies to confirm the presence of Ni(ii) in the catalyst. The catalyst was evaluated for its bi-functional activity towards the tandem conversion of benzaldehyde to ethyl benzoate and it was found that very small amounts of Ni (2.64 x 10(-3)mmol) enhance the selectivity towards benzoate. A detailed mechanistic study was carried out by UV-Visible and Raman spectroscopy to confirm that both intermediate species, Mo-peroxo and Ni-oxo, are responsible for higher selectivity towards esters. Further, a study to determine the effect of addenda atoms (heteropoly acid) was also carried out. The catalyst was also found to be viable for a number of aldehydes under optimized conditions.
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Reference:
Article; Weng, Shiue-Shien; Ke, Chih-Shueh; Chen, Fong-Kuang; Lyu, You-Fu; Lin, Guan-Ying; Tetrahedron; vol. 67; 9; (2011); p. 1640 – 1648;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics